Experimental Organic Chemistry
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|Author||: Philippa B. Cranwell,Laurence M. Harwood,Christopher J. Moody|
|Editor||: John Wiley & Sons|
The definitive guide to the principles and practice of experimental organic chemistry - fully updated and now featuring more than 100 experiments The latest edition of this popular guide to experimental organic chemistry takes students from their first day in the laboratory right through to complex research procedures. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures. The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis. The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over 100 validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills. New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry. New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis. Key aspects of this third edition include: Detailed descriptions of the correct use of common apparatus used in the organic laboratory Outlines of practical skills that all chemistry students must learn Highlights of aspects of health and safety in the laboratory, both in the first section and throughout the experimental procedures Four new sections reflecting advances in techniques and technologies, from electronic databases and information retrieval to semi-automated chromatography More than 100 validated experiments of graded complexity from introductory to research level A user-friendly experiment directory An instructor manual and PowerPoint slides of the figures in the book available on a companion website A comprehensive guide to contemporary organic chemistry laboratory principles, procedures, protocols, tools and techniques, Experimental Organic Chemistry, Third Edition is both an essential laboratory textbook for students of chemistry at all levels, and a handy bench reference for experienced chemists.
|Author||: John C. Gilbert,Stephen F. Martin|
|Editor||: Cengage Learning|
Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin's proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as small scale) and microscale users. The manual first covers equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book's experiments with confidence. Chapters show students how to use the book's techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
|Author||: Clark F. Most|
|Editor||: John Wiley & Sons Incorporated|
Acquaints students with all basic laboratory procedures, coordinating enough theory and technique to enable readers to fully comprehend the reactions being studied and the procedures involved. Material is organized in four sections: techniques, experiments, organic qualitative analysis, and appendixes. The first section introduces students to all common organic techniques and provides an illustrative experiment with each. A unique format helps train the research-oriented student to look for relationships that are not immediately apparent. The experiments section moves on to more complex experiments involving synthetic procedures followed by work-up and analysis requiring more than one technique. Instructions are complete and easy to follow, and a set of pre-laboratory experiments encourages students to determine goals before beginning lab work. The appendixes cover less-referred-to techniques: sublimation, density determination, and molecular weight determinations; and contaion a pronunciation guide and a compilation of chemical hazards.
|Author||: John C. Gilbert,Stephen F. Martin|
|Editor||: Cengage Learning|
Perform chemistry experiments with skill and confidence in your organic chemistry lab course with this easy-to-understand lab manual. EXPERIMENTAL ORGANIC CHEMISTRY: A MINISCALE AND MICROSCALE APPROACH, Sixth Edition first covers equipment, record keeping, and safety in the laboratory, then walks you step by step through the laboratory techniques you'll need to perform all experiments. Individual chapters show you how to use the techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. New experiments in Chapter 17 and 18 demonstrate the potential of chiral agents in fostering enantioselectivity and of performing solvent-free reactions. A bioorganic experiment in Chapter 24 gives you an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
|Author||: Charles F. Wilcox,Mary F. Wilcox|
|Editor||: Prentice Hall|
Takes a small scale approach to experimentation, keeping costs of material and their disposal down by a factor of five coompared to standard scale, while retaining most standard scale equipment and requiring no special glassware. The previous edition ISBN is: 0-02-427620-0.
|Author||: SONIA RATNANI,SHRINIWAS GURJAR|
|Editor||: PHI Learning Pvt. Ltd.|
Primarily intended for the undergraduate students of science, the book deals with the practical aspects of organic chemistry and discusses how experiments should be done in the laboratory. The book introduces the various types of components used in laboratories and describes basic techniques used for purification. It elaborates different methods of identification of organic compounds, their preparation, and analysis. In addition, it emphasizes qualitative analysis of organic compounds. The book contains essential experiments done in an organic lab and also explains the theoretical background of reactions involved. This book is an attempt to provide students with the often used methods in an easy to understand manner, including explanations of theory, procedures and interpretations of results of the experiments. Besides undergraduate students of science, this book is also useful for the postgraduate students of chemistry. KEY FEATURES : Includes reaction mechanism of each reaction Describes in Appendices safety measures to be taken in laboratory and how to prepare chemical reagents Contains self assessment questions at the end of each chapter.
|Author||: Carlos A M Afonso,Nuno R Candeias,Dulce Pereira Simão,Alexandre F Trindade,Jaime A S Coelho,Bin Tan,Robert Franzén|
|Editor||: Royal Society of Chemistry|
This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.
|Author||: Joaquín Isac-García,José A. Dobado,Francisco G. Calvo-Flores,Henar Martínez-García|
|Editor||: Academic Press|
Experimental Organic Chemistry: Laboratory Manual is designed as a primer to initiate students in Organic Chemistry laboratory work. Organic Chemistry is an eminently experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for future professionals to develop a strong background in the laboratory as soon as possible, forming good habits from the outset and developing the necessary skills to address the challenges of the experimental work. This book is divided into three parts. In the first, safety issues in laboratories are addressed, offering tips for keeping laboratory notebooks. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry. Organizes lab course coverage in a logical and useful way Features a valuable chapter on Green Chemistry Experiments Includes 84 experiments arranged according to increasing complexity
|Author||: Laurence M. Harwood,Christopher J. Moody,Jonathan M. Percy|
|Editor||: Blackwell Publishing|
This established text continues to provide a rigorous account of the principles and practice of experimental organic chemistry, taking students from their first day in the laboratory right through to research work. New to this edition, a microscale approach has been integrated into the entire text, alongside conventional manipulations, bringing it in line with current laboratory practice. Maintaining the unique structure of the previous edition, the first half of the book surveys all aspects of safe laboratory practice and the use of a wide range of purification and analytical techniques, particularly spectroscopic analysis. The second half contains easy-to-follow experimental procedures, each designed to illustrate an important reaction type of basic principle of organic chemistry. Tried and tested over the past decade, these experiments are graded according to their complexity and many of these have microscale equivalents. Of prime importance, all aspects of health and safety in the laboratory have been updated according to the latest guidelines and are highlighted throughout the text.
|Author||: John Gilbert,Stephen Martin|
|Editor||: Nelson Education|
Providing even more emphasis on inquiry-based learning, a new green experiment, and more than a dozen new discovery experiments, this Fifth Edition of Gilbert and Martin’s proven EXPERIMENTAL ORGANIC CHEMISTRY contains procedures for both miniscale (also known as small scale) and microscale users. The manual first covers equipment, record keeping, and safety in the laboratory, then walks students step by step through the laboratory techniques they need to perform the book’s experiments with confidence. Chapters show students how to use the book’s techniques to synthesize compounds and analyze their properties, complete multi-step syntheses of organic compounds, and solve structures of unknown compounds. A bioorganic experiment in Chapter 24 reflects the increasing emphasis on bioorganic chemistry in the course and gives students an opportunity to accomplish a mechanistically interesting and synthetically important coupling of two a-amino acids to produce a dipeptide. Important Notice: Media content referenced within the product description or the product text may not be available in the ebook version.
|Author||: Arun Sethi|
|Editor||: New Age International|
Basically The Book Has Been Written As A Textbook With An Intention To Serve The Students At The Graduate And Postgraduate Level. The Subject Matter Is Based On The New Model Curriculum Recommended By The University Grants Commission For All Indian Universities. The Book Provides An Exhaustive List Of Organic Compounds, Methods Of Its Identification, Its Derivatives Every Information Incorporated In Consolidated Form. Exercises Included In The Book Not Only Describe Different Methods/Techniques Of Preparation But Also Explain The Theoretical Background Of These Reactions. It Also Describes Different Methods Of Isolation Of Some Important Class Of Compounds. This Book Promotes Self Reliance Since It Is In Itself Complete Requiring No Reference To Other Texts.
|Author||: Addison Ault|
|Editor||: University Science Books|
Like its previous five editions, this book is ideally suited for use in a sophomore-level laboratory course in organic chemistry.Key Features of This Edition:Provides information on safety, glassware, lab cleanup, collection and disposal of waste, preparation of the laboratory notebook, and use of the chemical literature.Provides clear instructions on how to perform the procedures that are used.Appeals to the esthetic dimension by offering experiments in a variety of scales -from micro scale to semi-micro and to 5- and 10-gram scale.Includes descriptions of the interpretation of IR, UV/Vis, NMR and mass spectra.Gives procedures for the isolation of organic compounds from familiar materials such as nutmeg, cloves, citrus rind, tea, cola, NoDoz, aspirin, ibuprofen, milk and gallstones.Gives "recipes" for the preparation of organic compounds that illustrate many of the reactions that are discussed in the lecture part of the course.Gives procedures for the preparation of compounds with interesting properties: compounds that produce light, change color when heated, have different colors in different solvents, or turn blue in the sun.Includes the famous "bootstrap synthesis": the preparation of two molecules from one.Includes procedures for the preparation of 7 different compounds from vanillin.
|Author||: Jochen Mattay,Axel Griesbeck|
|Editor||: John Wiley & Sons|
Basic laboratory technique in organic chemistry plays a vital part in the education of chemistry students. This textbook contains a collection of multistep experiments that all feature one or two photochemical key steps. More than 40 researchers active in the field of organic photochemistry have contributed their favorite experiments for this unusual and modern textbook. In addition, a general section discusses reaction control, the interpretation of UV spectra, quantum yields and chemical yields, and gives information on solvents, lamps, filters, and vessels. The experiments chosen fulfil the following criteria: * starting materials are cheap and readily available * the necessary photochemical equipment is available in (most) institutes * products prepared are useful for further syntheses * the light reaction is efficient. 'Photochemical Key Steps' is a source book of new ideas for supervisors of lab courses and gives students the opportunity to learn about modern techniques in the laboratory and about the important role photochemistry plays in organic synthesis.